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Organometallic moieties such as ferrocene involved in conjugated systems like thiophene are of large interest as a foundation for the synthesis of organometallic polymers with the aim, among others, to obtain models for electron transfer models. It is known that ferrocenyl-containing compounds upon appropriate treatment produce magnetic nanoparticles, while polythiophene exhibits hole conduction, which is used to design optoelectronic and magnetic materials for various data storage devices, magnetic sensors, and magnetic elastomers. The aim of this work is to synthesis a new thiophene- and ferrocene-containing precursor for preparing ordered organohybrid assemblies to design new materials showing unique mechanical, electrical, optoelectronic, and paramagnetic properties.