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The study of the properties of filled elastomers is a challenging and exciting topic for both fundamental science and industrial application. It is known that adding of hard particulates to a soft elastomer matrix results in the properties that do not follow a straightforward rule of mixtures. In the present paper the microstructure properties of rubber elastomer matrix samples polymerized with ferrofluid and nanoparticles produced from Fe(CO)5thermal decomposition are investigated .by means of small-angle neutron and X-ray scattering experimental data using the fractals approach.