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In this work we compare the detection of various metal cations of tris(3-aminopropyl)amine derivatives; besides, chiral macrocyclic derivative of this tetraamine comprising endocyclic (S)-BINAM moiety was also studied as enantioselective fluorescence detector of model amino alcohols. The Pd(0)-catalyzed amination method for macrocyclization and the introduction of fluorophore groups has been widely used.