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Thus, by changing the atmosphere in which TiO2 NTs samples are annealed, it is possible to control the concentration of defects. Modification of the surface of TiO2 NTs samples with copperoxide nanoparticles stimulates the formation of oxygen radicals, which are involved in redox reactions, i.e., are responsible for the efficiency of photocatalysis. The prepared samples are promisingas photocatalysts.