Mechanochemical synthesis of vanadium(III) $\upbeta$-diketonatesстатья
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Дата последнего поиска статьи во внешних источниках: 17 апреля 2024 г.
Аннотация:The effect of the mechanical treatment conditions and of the nature of reactants on the course of thesolid-phase reaction of vanadium(III) chloride with sodium β-diketonates and potassium tetramethylheptanedionate, on the yield of the reaction products, and on some properties of the activated mixtures was examined. A method was developed for the synthesis of vanadium(III) β-diketonates by the solid-phase mechanochemicalreaction of vanadium(III) chloride with appropriate sodium or potassium β-diketonate, followed by sublimation or extraction.